Synthesis of New Derivative of Adipoyl Thiadiazole


This research includes the preparation of new derivatives of adipoyl thiadiazoles, through the reaction of each of hydrazine hydrate , phenyl hydrazine , 2,4-dinitrophenyl hydrazine, semicarbazide and thiosemicarbazid with adipoly chloride in the presence of ethanol (95%). Furthermore, thiadiazoles were made through cyclization of hydrazine , semicarbazide and thiosemicarbazid in alkaline media, such as potassium hydroxide solution in presence of carbon disulfide. The prepared compounds were identified by the physical and spectroscopic methods